Page 1 SOLA II Sulfur Online Analyzer User Guide P/N 90-1307-0 Revision Part of Thermo Fisher Scientific...
Page 2 SOLA II Sulfur Online Analyzer User Guide P/N 90-1307-0 Revision...
Page 3 © 2017 Thermo Fisher Scientific Inc. All rights reserved. “Teflon” is a registered trademark of E.I. du Pont de Nemours and Company. “Watlow” and “EZ-ZONE” are registered trademarks of Watlow Electric Manufacturing Company. “VICI is a registered trademark of Valco Instruments Co. Inc. and VICI AG. “Kaowool”...
Page 5: Revision History
Revised per ECO 7897. 02-2013 Revised per ECO 8126. 01-2014 Revised per ECO 8332. 11-2014 Revised per ECO 8545. 06-2016 Revised per ECO 8659. 06-2016 Revised per ECO 8667. Revised per ECO 8995. 01-2017 Thermo Fisher Scientific SOLA II User Guide...
Page 7: Table Of Contents
Installation Checklist ....................... 3-5 Chapter 4 Startup & Shutdown ..................4-1 Initial Startup ........................4-1 Startup after Short-Term Shutdown ................. 4-3 Short-Term Shutdown ....................4-4 Maintenance Shutdown ....................4-4 Emergency Shutdown ..................... 4-5 Thermo Fisher Scientific SOLA II User Guide...
Page 8 Chapter 9 At Line-Grab Sample ..................9-1 Safety Precautions ......................10-1 Chapter 10 Maintenance & Troubleshooting ..............10-1 Maintenance Schedule ....................10-1 Visual Inspection & Cleaning ..................10-2 Leak Tests ......................... 10-2 viii SOLA II User Guide Thermo Fisher Scientific...
Page 9 Troubleshooting ......................C-5 Appendix D TCP/IP Bridge ....................D-1 Hardware Configuration ....................D-1 Software Configuration ....................D-2 The Browser Interface ....................D-3 24 Hours Chart ......................D-4 24 Hours Table Format .................... D-4 Thermo Fisher Scientific SOLA II User Guide...
Page 10 PUVF Optical Bench ..................I-1 Appendix J Dual PMT Supply Option ................J-1 Overview ..........................J-1 Menu Changes for Dual PMT Supply Option ............J-2 Calibration Setup ......................J-2 AutoCal Setup ........................ J-3 Stream Setup ........................J-3 SOLA II User Guide Thermo Fisher Scientific...
Page 11 Connections ........................L-1 Connecting One Density Meter to a Dual Stream System ......L-3 Appendix M Related Technical Bulletins ................M-1 Appendix N Trace Level Measurements ................N-1 Appendix O Vapour Sample Measurements.................O-1 Thermo Fisher Scientific SOLA II User Guide...
Page 13: Safety Information & Guidelines
Failure to perform the instructions and procedures in this manual or other documents pertaining to this system correctly can result in equipment malfunction, equipment damage, and/or injury to personnel. Thermo Fisher Scientific SOLA II User Guide...
Page 14: Safety Summary
(e.g., detectors), or hot sample system components, appropriate gloves must be worn. Heated components should be allowed to cool before servicing if possible. Other appropriate equipment or clothing must be used as required by the type of work performed. SOLA II User Guide Thermo Fisher Scientific...
Page 15: Electrical Power
Warning Remove power prior to performing any work internal to the instrument. An override is available for use in non-hazardous areas; however, removal of components while the instrument is energized is not permitted. σ Thermo Fisher Scientific SOLA II User Guide 1-3...
Page 17: Chapter 2 Product Overview
(PUVF) detector. Unlike the original SOLA instrument, the PUVF is not a subassembly. The SOLA II is a single assembly with one software program and one user interface.
Page 18: Total Sulfur Measurement
The analyzer is equipped with a PUVF detector that accurately measures the quantity of SO formed during the combustion process. The SO molecules SOLA II User Guide Thermo Fisher Scientific...
Page 19 If the sample density varies significantly, a density correction is also λ necessary when using concentration units of ppm (w/w) or ppb (w/w). If using mg/L, ppm (w/v), ppm (v/v), ppb (w/v), or ppb (v/v), a density λ correction is not required. Thermo Fisher Scientific SOLA II User Guide 2-3...
Page 20: Principle Of Operation
UV light source. The measured SO concentration (representing total sulfur in the sample) is processed, displayed on the front panel display, and sent to the analog outputs. Figure 2–2. Typical functional flow diagram SOLA II User Guide Thermo Fisher Scientific...
Page 21: Puvf Detector
Thermo Fisher Scientific. The pyrolyzer typically operates at a temperature of 1100°C (2012°F) to oxidize sulfur without need for a catalyst. Figure 2–3. Pyrolyzer Thermo Fisher Scientific SOLA II User Guide 2-5...
Page 22: Dryer
Figure 2–4. Optional dryer Mixing Chamber The mixing chamber mixes the gases and permits the sample to vaporize to a gaseous state before entering the pyrolyzer. Figure 2–5. Typical mixing chamber SOLA II User Guide Thermo Fisher Scientific...
Page 23: Injection Valve
The sample then passes to the mixing chamber where it vaporizes (if necessary) and is thoroughly mixed with the air. See Appendix B for rotary injection valve service. Figure 2–6. Injection valve Thermo Fisher Scientific SOLA II User Guide 2-7...
Page 24: Specifications
Zone 1, G Ex pxb IIC T Gb (optional, X-Purge system; T3 and T4 optional with back-up purge system) II 3 G Ex pz IIC T3 Gc, SOLA II Flare or CV. T3 or T4 optional with back-up purge system, standard SOLA II...
Page 25 Analog signal load ≤ 600 ohms Inputs Dry contact; remote suspend, remote calibration, remote range select, remote stream select I/O ports Standard: RS485 Modbus RTU; RS485/RS232 Modbus Optional: TCP/IP encapsulated Modbus, browser-enabled interface Thermo Fisher Scientific SOLA II User Guide 2-9...
Page 26: Parts List
(Kalrez, Viton) Parts List The following table lists the SOLA II / SOLA II Trace parts. Note Unless otherwise specified, the parts listed below are for the SOLA II and the SOLA II Trace units. σ Table 2–5. SOLA II / SOLA II Trace parts list...
Page 27 Heater, wire sleeve, flameless burner TE-9886 Instrument cover 27-1068-0 49-1161-0 Keypad, numeric, 4-position 97-1580-0 Kit, TCP/IP Ethernet, Modbus 97-1403-0 Kit, valve inject TE-8666 Lamp, xenon, PUVF flash TE-8892 Lens assembly, detector, complete Thermo Fisher Scientific SOLA II User Guide 2-11...
Page 28 Malema flow switch kit 31-1354-0 Manifold assembly, 4-position with solenoid TE-8888 Mirror assembly, complete, SOLA II standard unit TE-57P746 Mirror assembly, dual, complete, SOLA II Trace unit TE-87420 Mirror, entrance 35-1527-0 Mounting bracket, TCP/IP PCB 97-1590-1 One-year spare parts kit, Dinfa valve, liquid phase applications...
Page 29 PCB, stream relay 89-2898-0 PCB, digital I/O TE-8684 Plate, filter lens TE-8868 PMT, SOLA II standard unit TE-8391 PMT, SOLA II Trace unit TE-8165 Power cord, 115 V 85-1173-0 Power supply, 110/220 Vac +5 V, ±12 V, for PCB, input option...
Page 30 27-1108-0 Thermocouple, S type TE-9934 Transducer, flow TE-9877 Transducer, pressure assembly TE-8774 Trigger pak for SOLA II bench, standard unit TE-8392 Trigger pak for SOLA II bench, Trace unit 30-1025-0 Tube, quartz pyrolyzer furnace, looped 64-1304-0 Tubing, 1/16”, Sulfinert 64-1051-0 Tubing, 1/16"...
Page 31: Spare Parts
Product Overview Spare Parts Spare Parts Table 2–6. SOLA II spare part kits Description 97-1589-0 Startup spare parts kit, Valco valve, liquid phase applications Qty. Includes Ferrules for pyrolyzer tube fittings, graphite Pyrolyzer tube, looped Pyrolyzer, O-ring 5 5/8” ID x 5 7/8” OD, 1/8” width Rotor, liquid sample valve, 1.0 µl, 4-port or 6-port...
Page 32 Thermocouple, pyrolyzer S type 10-port valve head, gas Rotor, 10-port, gas O-ring kit for liquid injection valve actuator UV flash lamp Filter, inline, 0.5 micron, 1/8” tube Valve, complete 10-port for gas 2-16 SOLA II User Guide Thermo Fisher Scientific...
Page 33 Pyrolyzer tube, looped Pyrolyzer, O-ring 5 5/8” ID x 5 7/8” OD, 1/8” width Thermocouple, pyrolyzer S type Slider block, 1.2 µl Filter, inline, 2 micron, 1/8” tube Filter, inline, 0.5 micron, 1/8” tube Thermo Fisher Scientific SOLA II User Guide 2-17...
Page 34 Critical operation spare parts kit, Dinfa valve, liquid phase applications Qty. Includes Solenoid relay PCB Valve, complete 8-port, 1.2 µl Optical bench assembly Pyrolyzer assembly Power supply board for SO bench Trigger pak Flasher supply board I/O PCB 2-18 SOLA II User Guide Thermo Fisher Scientific...
Page 35 Product Overview Spare Parts Table 2–7. SOLA II Trace spare parts kits 97-1592-3 Critical operation spare parts kit, Valco valve, liquid phase applications Qty. Includes Valve, inject, 1/16 6-port 1µl, 150 psi, 175°C Optical bench assembly Trigger pak, for SO...
Page 36 A/D PCB TE-8949 PUVF DC power supply board TE-8774 PUVF lamp trigger pak (consult factory for SOLA II Trace) TE-8884 PUVF flash intensity board (consult factory for SOLA II Trace) TE-9681 Flasher supply board (consult factory for SOLA II Trace)
Page 37: Storage
89-2897-0 89-2898-0 I/O PCB 85-1164-0 Power supply, 24 Vdc, DIN rail mount Storage If storing the instrument, the storage environment should be protected and free from extremes of temperatures and high humidity. Thermo Fisher Scientific SOLA II User Guide 2-21...
Page 39: Chapter 3 Installation
Caution This product is extremely heavy. Care must be taken at all times to avoid injury. Never attempt to move this product alone or without the use of lift gear. When handling the analyzer, ensure that all four corners are supported. σ Thermo Fisher Scientific SOLA II User Guide...
Page 40: Sample Line Installation
Caution Take necessary precautions to prevent exposure to hazardous materials when conditioning the sample tubing with sample. σ Proper preparation of sample tubing prior to installation is very important. Prepare the sample tubing as follows. SOLA II User Guide Thermo Fisher Scientific...
Page 41: Electrical Connections
2 A at 240 Vac or 10 A at 24 Vdc. Voltage is not supplied to the relay contacts by the analyzer. DCS & External The following inputs and outputs can be connected to a Distributed Control Connections System (DCS) or other devices as desired. Digital Inputs Thermo Fisher Scientific SOLA II User Guide 3-3...
Page 42: Optional Analog Inputs
Remote Control function must be enabled (“Analyzer Setup”, Chapter 6). Optional Analog Inputs Analog inputs are available for connecting densitometers used to correct each stream measurement based on the density of the sample. SOLA II User Guide Thermo Fisher Scientific...
Page 43: Analog Outputs
The following checklist may be copied for use during system installation. Checklist Details for the installation and various specification requirements are contained in this manual, application specific drawings, and information supplied with the instrument. Thermo Fisher Scientific SOLA II User Guide 3-5...
Page 44 AC power wiring is properly connected to the instrument with proper earth grounding. Signal wiring (DC signals, communications, etc.) meets requirements. Signal wires properly connected to the instrument. All electrical conduit seals poured with sealing compound such as Chico A5r or equivalent. SOLA II User Guide Thermo Fisher Scientific...
Page 45: Chapter 4 Startup & Shutdown
All sample lines to the analyzer MUST be cleaned and dried before initial use. c. Check all tubing connections to ensure they are tight and free of leaks. Pressure test the lines to check for leaks or use a liquid leak detector. Thermo Fisher Scientific SOLA II User Guide...
Page 46 Verify that the configuration settings in the menus match the application data sheet or system logbook. Suspend the analyzer (Chapter 5) to prevent accidental injection of sample while setting up the instrument. SOLA II User Guide Thermo Fisher Scientific...
Page 47: Startup After Short-Term Shutdown
2. Apply power to the analyzer. Note If the X-Purge option is installed, you must follow the instructions included in Appendix σ Thermo Fisher Scientific SOLA II User Guide 4-3...
Page 48: Short-Term Shutdown
Close the sample flow to the instrument and purge sample from the unit using air. 2. Turn off power to the analyzer. SOLA II User Guide Thermo Fisher Scientific...
Page 49: Emergency Shutdown
Caution Parts of the instrument may be hot even after power is removed. Allow the system to cool completely before performing maintenance. σ Emergency Close the sample supply to the system. Shutdown 2. Turn off the main power to the system. Thermo Fisher Scientific SOLA II User Guide 4-5...
Page 51: Chapter 5 Operation
4. Repeat the process used to enter the first digit for the remaining digits. 5. When you have completed this, press the button below Done. You can access all program features and edit parameters by following these steps. Figure 5–1. Thermo Fisher Scientific SOLA II User Guide...
Page 52: Begin Analyzing
3. To resume the analysis, go to the Analyzer Mode menu, and select Active. SOLA II User Guide Thermo Fisher Scientific...
Page 53: Injection Valve Failure Alarm
The diverter valves switch air to the injection valves under the following conditions: Injection Failure alarm λ Instrument power loss λ Instrument air loss λ Analysis suspension λ Thermo Fisher Scientific SOLA II User Guide 5-3...
Page 54 Operation Injection Valve Failure Alarm Figure 5–4. Sample diverter valves Figure 5–5. Sample diverter valves functional diagram SOLA II User Guide Thermo Fisher Scientific...
Page 55: Chapter 6 Configuration
Access the submenus within the Analyzer Setup menu by pressing Enter. Figure 6–2. 2. The first submenu is Program Passcode. The factory default is 0000. If the passcode remains 0000, you are not required to enter the passcode to Thermo Fisher Scientific SOLA II User Guide...
Page 56 60 seconds, the average concentration of the last 60 seconds is output at each update. Thus, lower averaging time means faster response to concentration changes. Longer averaging times are typically used to smooth output data. See the figure below. Figure 6–5. SOLA II User Guide Thermo Fisher Scientific...
Page 57 30, 60, 90, 120, 150, 180, 210, or 240 seconds. σ Figure 6–7. 7. There are three selections within this submenu: NONE, 4 to 20 mA, and Flow Switch. Thermo Fisher Scientific SOLA II User Guide 6-3...
Page 58: Stream Setup
3. If you select the Timed Stream option as the mode, you must determine the dwell time. Dwell time is the period of time the analyzer monitors one stream before it begins monitoring the other. Figure 6–11 displays the SOLA II User Guide Thermo Fisher Scientific...
Page 59 This period is called the purge time. In respect to calibration, purge time is how long the analyzer purges the line before it begins analyzing the calibration stream. You can set the purge time between 1 and 9999 seconds. See the figure below. Thermo Fisher Scientific SOLA II User Guide 6-5...
Page 60: Clock Setup
Access the Clock Setup menu to change the time and date. Figure 6–14. 2. Enter the time in hh:mm:ss, 24-hour format and the date (in the following screen) in mm/dd/yyyy format. Figure 6–15. Figure 6–16. SOLA II User Guide Thermo Fisher Scientific...
Page 61: Modbus Setup
3. Set the ID (network address) for Com 3. The address can be between 1 and 255. Figure 6–19. Set the baud rate and the ID for COM 4 in the same manner using the submenus for COM 4. Thermo Fisher Scientific SOLA II User Guide 6-7...
Page 62: Dual Range Setup
Figure 6–21. 2. The submenu shown below enables you to specify the full scale value (20 mA) for the high range of stream 1 as output on the 4–20 mA signal. Figure 6–22. SOLA II User Guide Thermo Fisher Scientific...
Page 63: Inject Setup
2. The injection time is the amount of time that the injection valve stays in the injection position. Set the inject time at half of the inject rate (1 to 9999 seconds). Figure 6–25. Thermo Fisher Scientific SOLA II User Guide 6-9...
Page 64: Autocal Setup
Figure 6–26. Autocal Setup Enter this menu to configure the autocal function. Figure 6–27. 2. The Autocal Mode submenu allows you to enable/disable periodic automatic calibration of the analyzer. Figure 6–28. 6-10 SOLA II User Guide Thermo Fisher Scientific...
Page 65 Access this submenu to specify this percentage. Note that an Autocal Fail alarm activates if the deviation exceeds the amount specified. See the figure below. Thermo Fisher Scientific SOLA II User Guide 6-11...
Page 66 Figure 6–32. 7. You can direct the reading during auto calibration to stream 1 or 2, 4–20 mA output, or none of the outputs. Figure 6–33. 6-12 SOLA II User Guide Thermo Fisher Scientific...
Page 67: Alarms Setup
3. To set up a Chamber Flow alarm, enter the set point at which the low flow alarm for the flow measured at the detector chamber in the PUVF should activate. The value can be from 0 to 1000 cc/m. Figure 6–36. Thermo Fisher Scientific SOLA II User Guide 6-13...
Page 68 1 to 50 V per 30 seconds. Figure 6–38. 6. Set up a Chamber Temperature alarm by entering the +/- deviation from 45°C at which the alarm should activate. Figure 6–39. 6-14 SOLA II User Guide Thermo Fisher Scientific...
Page 69 1 at which the alarm should activate. There are also submenus for setting the high alarm and the high high alarm for stream 2. If applicable, set these alarms as done for stream 1. Figure 6–42. Thermo Fisher Scientific SOLA II User Guide 6-15...
Page 70: Calibration
During normal operation, the average detector reading is interpolated on the line to derive the sulfur concentration reported. The graph below illustrates a SOLA II calibration. Figure 6–43. Prior to calibrating the instrument, the sulfur concentration expected at the two points must be entered in the calibration setup menus (Configuration >...
Page 71 High cal value = 100.00 ppm High cal = 15000.000 kHz Figure 6–44. Typical SOLA II calibration The high and low calibration can be performed independently. Changing either one of the calibration points will change the slope of the line. This is illustrated in the next two graphs.
Page 72 (see Figure 6–47). Enabling the Autocal function will cause the software to perform this correction automatically. Figure 6–47. Corrected calibration Several calibration functions can be performed. These are discussed in the following sections. 6-18 SOLA II User Guide Thermo Fisher Scientific...
Page 73: Performing A Low Calibration At Zero
*No injections Calibration at Zero* Note This is the most common form of low calibration that requires only one standard. For SOLA II Trace, it is recommended that a low concentration standard be used. σ Note To prevent repetition, these sections do not include screen shots. Each menu item within the Calibration Setup menu is shown in “Calibration Setup...
Page 74: Performing A High Calibration
(readings are performed once a second). The resulting average will be latched to correspond to the high calibration value concentration. The Recalibrate High Function 6-20 SOLA II User Guide Thermo Fisher Scientific...
Page 75: Adjusting The Reading
At this point, the current average of the detector signal is latched to correspond to the high calibration value concentration. Adjusting the If the reported value of the SOLA II does not match a known sample value or Reading the standard flowing through the instrument, you can adjust the reading. To do so, go to Configuration >...
Page 76: Calibration Setup Menu Items
Select the engineering unit related to the concentration entered for the calibration values: ppm, ppb, or mg/L. Figure 6–49. 2. Enter the concentrations of the high calibration standard. See “Performing a High Calibration” for more. Figure 6–50. 6-22 SOLA II User Guide Thermo Fisher Scientific...
Page 77 4. Set the number of readings the analyzer should average during calibration (1–60 readings). Figure 6–52. 5. Begin a calibration for the high concentration standard. See “Performing a High Calibration” for more. Figure 6–53. Thermo Fisher Scientific SOLA II User Guide 6-23...
Page 78 8. Adjust calibration during operation to match lab results through the Adjust Reading menu item. Enter a concentration, and the reading is forced to match the value entered. See “Adjusting the Reading” for more. Figure 6–56. 6-24 SOLA II User Guide Thermo Fisher Scientific...
Page 79: Density Compensation Setup
If no correction is desired, set the correction factor to 1.000. The following provides instructions for both methods. If using a densitometer, refer to the instructions with Figures 6–59 through 6–63. Menu items for stream 1 are used. Thermo Fisher Scientific SOLA II User Guide 6-25...
Page 80 2. Select Live. If you are using stream 2, be sure the menu item is for stream Figure 6–60. 3. Enter the density of the calibration standard (in units of g/cc). Figure 6–61. 6-26 SOLA II User Guide Thermo Fisher Scientific...
Page 81 The following provides instructions on entering a correction factor using stream 2. Select Fix in the Str2 Compensation menu item. If using stream 1, be sure the menu item is for stream 1. Figure 6–64. Thermo Fisher Scientific SOLA II User Guide 6-27...
Page 82 2. Enter the correction factor. The value may be from 0 to 9.999. Figure 6–65. Note that when using a correction factor, you do not need to enter the Cal Density menu. 6-28 SOLA II User Guide Thermo Fisher Scientific...
Page 83: Chapter 7 Viewing Alarms
The second top-level menu is the View/Ack Alarm menu. Figure 7–1. Access this menu to review all active alarms. Use the up and down arrows to scroll through the alarms individually. Press Ack to acknowledge the alarm. Figure 7–2. Thermo Fisher Scientific SOLA II User Guide...
Page 85: Chapter 8 Diagnostics
Figure 8–2. Set Outputs In the Set Outputs group, press Tgle to toggle the associated relay on and off. Figure 8–3. Following are the relays that can be accessed through the Set Outputs group. Thermo Fisher Scientific SOLA II User Guide...
Page 86: View Mux Analogs
Reserved for factory test only; the 2 pound signs (##) indicate the control output. Note Solenoids 7 and 8 are reserved for future applications and are not installed in the standard unit. σ View MUX Analogs SOLA II User Guide Thermo Fisher Scientific...
Page 87: View 4-20 Ma Inputs
3. ADC 7 Pressure 4. ADC 9 PMT V 5. ADC 10 Chamber T 6. ADC 11 Ambient T View 4–20 mA Inputs Access this submenu to view the optional 4–20 mA inputs. Figure 8–5. Thermo Fisher Scientific SOLA II User Guide 8-3...
Page 88: View Digital Inputs
Displays the status of stream select switch #2 Range Control Displays the status of the range control switch Remote Cal Displays the status of the remote calibration switch Remote Suspend Displays the status of the remote suspend switch SOLA II User Guide Thermo Fisher Scientific...
Page 89: View Parameters
(calculated at 0 concentration). Working Average Sec When switching from the normal average to the fast average and back to normal, the average time used can be observed from this menu item. Thermo Fisher Scientific SOLA II User Guide 8-5...
Page 90: View Com Activity
Lamp Voltage The lamp input voltage. Stream 1 Density The density of stream 1. Stream 2 Density The density of stream 2. View Com This menu displays activity for Coms 1–4. Activity Figure 8–9. SOLA II User Guide Thermo Fisher Scientific...
Page 91: Pulse Uv Control
Change the duration of the sample portion of the sample and hold Hold Time) analog front end (normally 100 µs). (Sample portion is the amount of time the sample and hold device is in the SAMPLE state.) Thermo Fisher Scientific SOLA II User Guide 8-7...
Page 93: At Line-Grab Sample
ID is programmed. Figure 9–1. 2. Average sampling time is the number of seconds that the sample is averaged to compute the result. It can be between 60 and 240 seconds. Figure 9–2. Thermo Fisher Scientific SOLA II User Guide...
Page 94 If it is greater than the programmed value, an error is reported. Figure 9–3. Activate the function from the front panel or the SOLA web interface. Figure 9–4. Figure 9–5. At line sampling screen SOLA II User Guide Thermo Fisher Scientific...
Page 95: Safety Precautions
Replace the injection valve rotor or slider according to Appendix Annually Test the instrument for internal leaks as explained later in this chapter. Every 18 months Replace the pyrolyzer heater as explained later in this chapter. Thermo Fisher Scientific SOLA II User Guide 10-1...
Page 96: Visual Inspection & Cleaning
Check the system fittings with a liquid or electronic leak detector. c. Correct any leakage. d. Repeat the leak test. 7. When the system passes the leak test, adjust the sample and air regulators fully counterclockwise to close supply flows. 10-2 SOLA II User Guide Thermo Fisher Scientific...
Page 97: Flow Rate Checks
3. Ensure that the analyzer is stabilized at normal operating temperatures before proceeding. Suspend the analyzer according to Chapter 5. Thermo Fisher Scientific SOLA II User Guide 10-3...
Page 98: The Rotary Valve
3. Loosen the screw located in the center of the bracket holding the mixing chamber to the bottom of the enclosure. 4. Carefully slide the mixing chamber from the bracket. Note Install the mixing chamber by following the above steps in reverse. σ 10-4 SOLA II User Guide Thermo Fisher Scientific...
Page 99: Replacing The Pyrolyzer Heater
The following table lists the part numbers for the parts referenced in this procedure. With the exception of the heater being replaced, the existing parts can be reused if in good condition. The part numbers are provided here for convenience. Thermo Fisher Scientific SOLA II User Guide 10-5...
Page 100 Do not discard the mounting screws. You will need them later. 7. Remove the six screws and washers from the lid of the housing (Figure 10- 3). Set them aside for later use. 10-6 SOLA II User Guide Thermo Fisher Scientific...
Page 101 Remove the heater wires from the terminal block and straighten the wires. Remove the fiberglass insulation that covers the heater wires (Figure 10-6). Set the insulation aside. You will need it later. Thermo Fisher Scientific SOLA II User Guide 10-7...
Page 102 12. You should now be able to remove the heater from the housing. 13. Insert the replacement heater into the housing (Figure10-7). Feed the two heater wires through the two fittings on the other side of the housing (Figure 10-8). 10-8 SOLA II User Guide Thermo Fisher Scientific...
Page 103 Figure 10–7. Insert replacement heater into housing Figure 10–8. Heater wires fed through fittings 14. Slide the wire sleeves onto the heater wires. Tighten the stainless steel fittings (Figure 10-9). Figure 10–9. Wire sleeves and fittings Thermo Fisher Scientific SOLA II User Guide 10-9...
Page 104 3/8” exposed (Figure 10-11). Figure 10–11. Add the fiberglass insulation 17. Insert the ends of the heater wires into the terminal block and tighten them. Bend the wires as shown in Figure 10-12. 10-10 SOLA II User Guide Thermo Fisher Scientific...
Page 105 21. With an air gun placed at the end of one fitting, blow out any dust or debris that may have dropped inside the pyrolyzer quartz or glass tube (Figure 10-13). Thermo Fisher Scientific SOLA II User Guide 10-11...
Page 106 23. If necessary, reconnect the wires from the oven temperature switches. 24. Reconnect the heater wires to the pyrolyzer. 25. Reconnect the thermocouple wires. 26. Reconnect the sample tubing. 27. Follow the initial startup procedure in Chapter 4 to restart the analyzer. 10-12 SOLA II User Guide Thermo Fisher Scientific...
Page 107: The Pyrolyzer Reaction Tube
Set the fittings, insulation, and Kaowool insulation aside for use in the next steps. 4. Carefully push both ends of the replacement pyrolyzer tube through holes of the insulation (Figure 10-16). Thermo Fisher Scientific SOLA II User Guide 10-13...
Page 108 See Figure 10- Figure 10–18. Reattach the ferrules and fittings 7. Gently slide the lid back into the housing and secure it using the screws and washers removed earlier. 10-14 SOLA II User Guide Thermo Fisher Scientific...
Page 109: Decoking
Carbon built up in the reaction tube absorbs SO , resulting in poor instrument performance and invalid results. Note We do not recommend decoking the tube. Instead, replace the tube according to the previous section. σ General Troubleshooting Thermo Fisher Scientific SOLA II User Guide 10-15...
Page 110 If it becomes necessary to contact Thermo Fisher Scientific with software or hardware problems, please have the following information available: Valve type λ Sample composition λ Options installed λ Ranges λ 10-16 SOLA II User Guide Thermo Fisher Scientific...
Page 111 - Ambient temperature or purge air is - Measure ambient and purge air temperatures and View/Ack Alarm menu) outside ambient temperature limits correct as necessary. - Thermistor not positioned correctly - Reposition Thermistor. Thermo Fisher Scientific SOLA II User Guide 10-17...
Page 112 Replace with known good lamp to see if problem is resolved. Lamp trigger pak Replace. Low lamp intensity Flasher lamp Ensure lamp and trigger pak are securely fastened. Fault on the I/O PCB. 10-18 SOLA II User Guide Thermo Fisher Scientific...
Page 113: Contact Information
+86 (10) 8419-3580 fax Ion Path, Road Three Winsford, Cheshire CW7 3GA UNITED KINGDOM +44 (0) 1606 548700 +44 (0) 1606 548711 fax www.thermoscientific.com For returns, contact Thermo Fisher Scientific for specific instructions. Thermo Fisher Scientific SOLA II User Guide 10-19...
Page 114: Warranty
Maintenance & Troubleshooting Warranty Thermo Scientific products are warranted to be free from defects in material Warranty and workmanship at the time of shipment and for one year thereafter. Any claimed defects in Thermo Scientific products must be reported within the warranty period.
Page 115: Appendix A Watlow Ez-Zone ® Pm6 Series
Display & Keys The display and keys on the EZ-ZONE PM6 are shown below and described in the table that follows. Figure A–1. EZ-ZONE PM6 series controller Thermo Fisher Scientific SOLA II User Guide A-1...
Page 116 When in the Home page, use the Up and Down keys to adjust the set point in the lower display. When in other pages, use the keys to change the upper display to a higher or lower value or to change a parameter selection. SOLA II User Guide Thermo Fisher Scientific...
Page 117: Software Configuration
Caution! Changing the parameters may adversely affect the system performance. σ The default settings for the pyrolyzer are provided in the tables on the Pyrolyzer Settings following pages. Table A–2. Pyrolyzer settings: Setup Page > Analog Input 1 Thermo Fisher Scientific SOLA II User Guide...
Page 118 The minimum value of the open loop set point range. Set Point Open Limit High 100.0% The maximum value of the open loop set point range. Table A–4. Pyrolyzer settings: Setup Page > Output 1 SOLA II User Guide Thermo Fisher Scientific...
Page 119 Deviation Alarm Alarm Hysteresis 2°C Alarm Logic Open On Alarm The output condition during an alarm state. Alarm Sides Both Both high and low sides can trigger the alarm. Alarm Latching Non-Latching Alarm Blocking Thermo Fisher Scientific SOLA II User Guide...
Page 120 The Channel LED is on. Display Pairs The number of display pairs. Display Time The time delay for toggling between channel 1 and channel 2. User Settings Save None User Settings Restore None SOLA II User Guide Thermo Fisher Scientific...
Page 121 Ambient Error RTD Error Not Sourced Calibration Offset The offset applied to the input reading to compensate factors that cause the input reading to vary from the actual process value (°C). Default = 0. Thermo Fisher Scientific SOLA II User Guide...
Page 122 Cool Proportional Band 14°C The PID proportional band for the cool outputs. Cool Hysteresis 2°C The process value needs to be this far into the “on” region before the output turns on. SOLA II User Guide Thermo Fisher Scientific...
Page 123 Table A–14. Pyrolyzer settings: Factory Page > Custom Setup 2 Parameter Default Comment Display Software Display Software Parameter Active Set Point The parameter that will appear in the custom Home Page. Instance ID Thermo Fisher Scientific SOLA II User Guide...
Page 124 The security level of the Operations Page. Password Enable Read Lock The level of read security clearance. Write Security The level of write security clearance. Locked Access Level Rolling Password User Password Administrator Password A-10 SOLA II User Guide Thermo Fisher Scientific...
Page 125: Oven Settings
-18.0°C The output low range. Range High 5537.0°C The output high range. Process Error Enable Process Error Low Value 0.00 Filter For smoothing the process signal. Input Error Latching Display Precision Tenths Thermo Fisher Scientific SOLA II User Guide A-11...
Page 126 High Set Point 200.0°C The maximum value of the closed loop set point range. Set Point Open Limit Low -100.0% The minimum value of the open loop set point range. A-12 SOLA II User Guide Thermo Fisher Scientific...
Page 127 Software Alarm Type Deviation Alarm Alarm Hysteresis 2°C Alarm Logic Open On Alarm The output condition during an alarm state. Alarm Sides Both Both high and low sides can trigger the alarm. Thermo Fisher Scientific SOLA II User Guide A-13...
Page 128 The Channel LED is on. Display Pairs The number of display pairs. Display Time The time delay for toggling between channel 1 and channel 2. User Settings Save None User Settings Restore None A-14 SOLA II User Guide Thermo Fisher Scientific...
Page 129 Software Control Mode Active The control mode currently in effect. Possible displays listed below. Auto Manual Heat Power The current heat output level (%). Cool Power The current cool output level (%). Thermo Fisher Scientific SOLA II User Guide A-15...
Page 130 The offset to the proportional band. Open Loop Set Point 0.0% The fixed level of output power when in manual (open loop) mode. Table A–27. Oven settings: Operations Page > Alarm 1 A-16 SOLA II User Guide Thermo Fisher Scientific...
Page 131 The parameter that will appear in the custom Home Page. Instance ID Table A–31. Oven settings: Lock Page > Lock 1 Parameter Default Comment Display Software Display Software Operations Page The security level of the Operations Page. Thermo Fisher Scientific SOLA II User Guide A-17...
Page 132: The Lockout Menu
You can change the read and write access to these Menu menus and pages through the Lockout menu [LoC]. These security functions are described in detail in the EZ-ZONE PM PID Controller user’s manual. A-18 SOLA II User Guide Thermo Fisher Scientific...
Page 133: Appendix B Rotary Valve Service
Note If other tubing is to be used, make certain that all tubing ends are free of burrs and cut square with the tube axis, and that all tubing has been cleaned chemically and mechanically. σ Thermo Fisher Scientific SOLA II User Guide B-1...
Page 134: Valve Disassembly
As this figure illustrates the valve can be disassembled for cleaning and/or rotor replacement without removing the loops and tubing from the valve or removing the valve from the actuator or mounting bracket. SOLA II User Guide Thermo Fisher Scientific...
Page 135: Cleaning The Valve Body
If any scratches are visible between the ports or anywhere that might suggest a potential leakage path or wear source, the valve should be returned to the factory for grinding and polishing. Thermo Fisher Scientific SOLA II User Guide...
Page 136: Cleaning The Rotor
Note Make certain that the valve is never left partially actuated. It should always be in either its fully clockwise or fully counterclockwise position. σ SOLA II User Guide Thermo Fisher Scientific...
Page 137: Conditioning Procedure For High Temperature Valves
Temperature carrier gas (oxygen-free) flowing through all the ports, rapidly heat the valve to 325°C. When this temperature is reached, cycle the valve 10 times and let it Valves cool to operating temperature. Thermo Fisher Scientific SOLA II User Guide...
Page 138: Two-Position Air Actuator O-Ring Replacement
CR3/clamp ring on the actuator. b. Pull off the standoff with the valve attached. c. Use the 9/64” hex driver to remove the two HWSC-SC8-6/socket-head screws that hold the clamp ring to the actuator. SOLA II User Guide Thermo Fisher Scientific...
Page 139 The procedures are the same for either type.) 8. Loosen but do not remove the three slotted head screws that hold the subassembly together. Thermo Fisher Scientific SOLA II User Guide...
Page 140 2. Use a lint-free tissue to clean the O-ring grooves as completely as possible. 3. Upon installation, coat each new O-ring with a thin layer of Dow Corning DC-111 (or similar silicone lubricant). Figure B–9. Locations of O-rings SOLA II User Guide Thermo Fisher Scientific...
Page 141: Assembly
6. Install the three end cap screws with the PEEK washers provided. Thermo Fisher Scientific SOLA II User Guide...
Page 142: Valve Alignment
6. Repeat the visual inspection. If the steps have been executed correctly, the rotor pin should contact the stops in both positions. If it does not, repeat the entire procedure. Follow these steps to rebuild the subassembly: B-10 SOLA II User Guide Thermo Fisher Scientific...
Page 143: Rebuild The Assembly
Tighten the screws in rotation to insure optimum alignment. 10. Pull the subassembly off the male end cap so that its orientation can be checked, and proceed with step 2 of “Assembly”. Thermo Fisher Scientific SOLA II User Guide B-11...
Page 144 Rotary Valve Service Rebuild the Assembly Figure B–12. Exploded view of two-position actuator B-12 SOLA II User Guide Thermo Fisher Scientific...
Page 145: Appendix C Dinfa Valve Service
Appendix C Dinfa Valve Service Overview Figure C–1. Dinfa valve mounting & parts locator Figure C–2. Position of heat transfer tube in oven Thermo Fisher Scientific SOLA II User Guide C-1...
Page 146 Figure C–3. Dinfa 8-port liquid injection valve, sample load position Note To set up two injections/minute, set the injection cycle to 30 sections and the injection time to 15 seconds. σ Figure C–4. 8-port liquid injection valve, inject position SOLA II User Guide Thermo Fisher Scientific...
Page 147 3. Set the make-up air (clean air 1) to 60 psig. 4. Allow the oven and pyrolyzer temperatures to stabilize at 190°C and 1100°C, respectively. 5. Apply sample and observe the results. Do not exceed 50 psig of sample pressure. hermo Fisher Scientific SOLA II User Guide...
Page 148 Dinfa Valve Service Overview Figure C–6. Dinfa 8-port liquid injection valve Figure C–7. Close-up of slider SOLA II User Guide Thermo Fisher Scientific...
Page 149: Troubleshooting
The heat transfer tube is not insulated properly, or there is λ insufficient clean airflow through the valve. The clean air tubing from the oven to the Dinfa valve is not properly λ insulated. Figure C–8. Valve block tension adjustment bolts hermo Fisher Scientific SOLA II User Guide...
Page 151: Appendix Dtcp/Ip Bridge
Appendix D TCP/IP Bridge The SOLA II Modbus TCP/IP option is a microprocessor-driven board that provides a bridge between the SOLA II standard serial Modbus and a TCP/IP Modbus network using 10 Base-T. Hardware TCP/IP Bridge board installed inside the SOLA II enclosure λ...
Page 152: Software Configuration
4. Record the IP address assigned to the bridge. This is the IP address required for configuring a workstation or DCS to query the SOLA II. On the TCP/IP Modbus frame, the unit ID must always be set to 1.
Page 153: The Browser Interface
“http://” followed by the IP address into the address line of the browser. For example, if the IP address is 10.209.64.145, enter “http://10.209.64.145” into the address line. The SOLA II TCP/IP Bridge main page opens (Figure D–4). The main page displays the status of the instrument and refreshes every 15 seconds.
Page 154: 24 Hours Chart
Figures D–6 through D–14 display the parameters you can access from a remote location by clicking Configuration. If the passcode is not 0000, you must enter the correct passcode to change the parameters. Click Apply to save the changes. SOLA II User Guide Thermo Fisher Scientific...
Page 155 TCP/IP Bridge The Browser Interface Figure D–6. Analyzer setup Figure D–7. Stream setup Figure D–8. Modbus setup Thermo Fisher Scientific SOLA II User Guide...
Page 156 TCP/IP Bridge The Browser Interface Figure D–9. Dual range setup Figure D–10. Inject setup Figure D–11. Autocal setup SOLA II User Guide Thermo Fisher Scientific...
Page 157 TCP/IP Bridge The Browser Interface Figure D–12. Alarm setup Figure D–13. Calibration setup Figure D–14. Density compensation setup Thermo Fisher Scientific SOLA II User Guide...
Page 158: At Line Sample
PC that is running the web browser. Figure D–15. At line grab sample form Complete this form and click Start Sample to begin the sampling process. Figure D–16. Sampling in process SOLA II User Guide Thermo Fisher Scientific...
Page 159 TCP/IP Bridge The Browser Interface Figure D–17. Sample results Thermo Fisher Scientific SOLA II User Guide...
Page 161: Appendix E Version 1.20 Modbus Registers
Table E–2. (0)0040 Coil Number Description Enable Modbus Remotes Stream Select 0 Stream Select 1 Reserved Remote Low Cal Remote High Cal Remote Suspend Remote Autocal Alarm Ack Reserved Reserved Reserved Reserved Thermo Fisher Scientific SOLA II User Guide E-1...
Page 162: Coils (0)0001 To (0)0040
If the coil is set to 0 (default power-on condition), the rest of the coils are ignored, and the remote functions are controlled by the digital inputs. Same function as the remote stream select digital inputs. SOLA II User Guide Thermo Fisher Scientific...
Page 163: Status Inputs (1)0001 To (1)0025
Grab Sample Ended 10019 Reserved 10020 Reserved 10021 Reserved 10022 Reserved 10023 Reserved 10024 Reserved 10025 Reserved Note: Stream 1 = Reg 30001/32768 * Reg 30003 Stream 2 = Reg 30002/32768 * Reg 30004 Thermo Fisher Scientific SOLA II User Guide...
Page 164: Input Registers (3)0001 To (3)0040
30019 Last Autocal Deviation % 30020 Bench Chamber Flow 30021 Bench Pressure (*10) 30022 Density 1 g/cc *1000 30023 Density 2 g/cc *1000 30024 Reserved 30025 Reserved 30026 Reserved 30027 Reserved 30028 Reserved SOLA II User Guide Thermo Fisher Scientific...
Page 165: Holding Registers (4)0001 To (4)0049
High Alarm 1 (*10) 40011 High High Alarm 1 (*10) 40012 High Alarm 2 (*10) 40013 High High Alarm 2 (*10) 40014 Stream Mode Select: 0 = auto, 1 = stream 1, 2 = stream 2 Thermo Fisher Scientific SOLA II User Guide...
Page 166 Chamber Temperature Alarm Set Point 40037 Average Cal Reads 40038 Alarm Mode 40039 Range Mode 40040 Autocal Mode 40041 Stream 1 Density Live 40042 Stream 2 Density Live 40043 Com 3 Baud Rate 40044 Com 3 ID SOLA II User Guide Thermo Fisher Scientific...
Page 167 Stream 1 Flow: 1 = High, 0 = Low 40053 Stream 2 Flow: 1 = High, 0 = Low 40054 Autocal Value 40055 Cal 4-20 mA Output: 0 = none, 1 = Stream 1, 2 = Stream 2 4-20 Thermo Fisher Scientific SOLA II User Guide...
Page 169: Appendix F The Workstation
Appendix F The Workstation Installing The SOLA II workstation software is an application developed to run under Workstation National Instruments™ Lookout. The software consists of the following items: Software Lookout Development System λ Floppy disk with a subdirectory named SOLA containing the following λ...
Page 170 Select Object > Modify > Modbus1 (Figure F–1). c. Edit the Modbus object to select a different COM port or Modbus Ethernet (Figure F–2). Figure F–1. Figure F–2. 5. If Mode is set to Modbus Ethernet: SOLA II User Guide Thermo Fisher Scientific...
Page 171: Workstation Operation
Note The specified Receive gap, RTS delay, and CTS time-out are critical to achieve successful communication with the analyzer. Depending on the PC used, these numbers may need to be increased. σ Figure F–3. Workstation Operation Thermo Fisher Scientific SOLA II User Guide...
Page 172 Note The workstation collects real-time data from the analyzer. For proper operation, the workstation should be run continuously with a connection to the analyzer. σ SOLA II User Guide Thermo Fisher Scientific...
Page 173: Statistics
The Stream Plot area displays the trend of measured total sulfur for stream 1 and stream 2 (if second stream option is installed on the analyzer). The currently active stream is indicated by a green indicator on that stream name Thermo Fisher Scientific SOLA II User Guide...
Page 174: Detector Status
Figure F–6. Detector status screen Alarms Status If an alarm, fault, or malfunction is detected, the indicator on the Alarms Status button turns red. Clicking Alarms Status displays a list of the alarms SOLA II User Guide Thermo Fisher Scientific...
Page 175: Remote Controls
Values in the Allowed Deviation and Recal Deviation determine whether the calibration factor is updated to the new value. 3. Remote Suspend: When turned on, analyzer operation is suspended. When turned OFF, the analyzer functions normally. Thermo Fisher Scientific SOLA II User Guide...
Page 176: Analyzer Status
Setup, Calibration Setup, Autocal / Validation Setup Stream Setup. Note The analyzer workstation operation and configuration applications must not be run simultaneously. If running, always close the configuration application before opening the operation application. σ Figure F–9. SOLA II User Guide Thermo Fisher Scientific...
Page 177: Appendix G The X-Purge System
A flame arrestor is also installed between each pressure differential switch and the associated pressure enclosure that it monitors. A spark arrestor vent is used for exhaust purposes. It also maintains appropriate backpressure on the electronics enclosure and oven. Thermo Fisher Scientific SOLA II User Guide G-1...
Page 178 σ Note Blanking elements or plugs used shall be in accordance with national standards. σ Figure G–1. Purge control unit (ATEX version shown. NFPA version has key switch inside enclosure) SOLA II User Guide Thermo Fisher Scientific...
Page 179: X-Purge Specifications
Utility requirements Instrument air 60–80 psig, 8 SCFM (maximum) Instrument air quality Water and oil free, -40°C (-40°F) dew point, particles < 5µ, ISA grade, hydrocarbon free AC power 110 Vac, 50/60 Hz Thermo Fisher Scientific SOLA II User Guide...
Page 180: Installation
AC power connections to the X-Purge unit. Table G–1. Power Terminal TB1-1 Neutral TB1-3 Ground TB1-5 Power out (switched) TB1-6 Terminals 1 and 2 are jumpered together. Terminals 3 and 4 are jumpered together. SOLA II User Guide Thermo Fisher Scientific...
Page 181: Alarm Signal
2. Open the instrument air supply to the analyzer. 3. Close the oven door securely and adjust the oven air pressure regulator to the value required for the analyzer (refer to the application notes or logbook for the analyzer). Thermo Fisher Scientific SOLA II User Guide...
Page 182: Shutdown
2. Remove power to the X-Purge system. 3. Complete the remaining shutdown steps listed in the applicable shutdown procedure in the instrument user’s guide. SOLA II User Guide Thermo Fisher Scientific...
Page 183: Power Or Purge Loss Shutdown
Do not leave the analyzer system unattended when the NORMAL / BYPASS switch is in the BYPASS position. Personnel must remove power from the system immediately if hazardous conditions are suspected. σ Thermo Fisher Scientific SOLA II User Guide...
Page 184: Timer Adjustment
32 are ON, the time delay is 8 minutes (i.e. 256 + 128 + 64 + 32 = 480 seconds). When replacing the time delay relay, the switches on the new relay must be set the same as on the relay being replaced. SOLA II User Guide Thermo Fisher Scientific...
Page 185: Appendix H Software Menu Tree
Appendix H Software Menu Tree Figure H–1. Top-level menus & configuration subgroups Thermo Fisher Scientific SOLA II User Guide H-1...
Page 186 Software Menu Tree Figure H–2. Diagnostics subgroups SOLA II User Guide Thermo Fisher Scientific...
Page 187: Appendix Ipuvf Optical Bench
Appendix I PUVF Optical Bench Figure I–1. Optical bench assembly exploded diagram Thermo Fisher Scientific SOLA II User Guide I-1...
Page 189: Appendix J Dual Pmt Supply Option
8000 ppm S w/w was set up with a PMT voltage of -570 Vdc, and a SOLA II calibrated for a full scale range of 10 ppm S w/w was set up with a PMT voltage of -950 Vdc.
Page 190: Menu Changes For Dual Pmt Supply Option
Note that the analyzer will not update readings during this period. Menu Changes The Dual PMT Supply option requires a different version of the SOLA II for Dual PMT software installed in the unit to operate properly. The software introduces several changes to the standard configuration menus.
Page 191: Autocal Setup
(20 mA) is configurable for each calibration. Calibration A Range: Enter the 20 mA value. 2. Calibration B Range: Enter the 20 mA value. Diagnostics Display Thermo Fisher Scientific SOLA II User Guide...
Page 192: At Line-Grab Sample
The dual PMT supply option can be retrofitted to existing units in the field. The parts in the table below are required for the field retrofit. Table J–1. Description 98-1049-0 SOLA II Dual Cal software 97-1649-0 SOLA II Dual PMT Supply kit SOLA II User Guide Thermo Fisher Scientific...
Page 193 GB/T26572-2011 有毒有害物质名称及含量的标识格式有毒有害物质或元素 (SOLA-II) 部件名称铅汞镉六价铬多溴联苯多溴二苯醚（Pb）（Hg）（Cd）（Cr6+）（PBB）（PBDE）外壳 CPU 电路板可移动的卡片量具组件温度控制器条带监测器传感器组熔炉交流/直流配电电源缆线连接 ○：表示该有毒有害物质在该部件所有均质材料中的含量均在GB/T26572-2011标准规定的限量要求以下表示该有毒有害物质至少在该部件的某一均质材料中的含量超出GB/T26572-2011标准规定的限量要求 Thermo Fisher Scientific SOLA II User Guide...
Page 195: Purpose
In the figure below, note that terminals 2 and 4 of the Sarasota FD910 density meter are connected to the return of the SOLA II supply loop. It is acceptable to run three wires between the devices and jumper terminals 2 and 4 together at the density meter and connect either terminal 2 or terminal 4 of the density meter to terminal 3 of the SOLA II 4–20 mA inputs.
Page 196 If the jumper is installed, the 24VDC current loop power is supplied by the SOLA II. If the jumper is left open, power is not supplied by the SOLA II. For the Sarasota FD910, an external current loop power supply is required, so the jumper needs to be installed for each channel using the density meter as an input.
Page 197: Connecting One Density Meter To A Dual Stream System
Density Meter to a Note The jumper for loop power is NOT installed for stream 2 (J9). Dual Stream System σ Figure L–5. Sarasota FD910 density meter to SOLA II dual stream system connections Thermo Fisher Scientific SOLA II User Guide...
Page 199: Appendix M Related Technical Bulletins
This appendix provides a list of technical bulletins related to this product as of the release date of this document revision. For the most current bulletins, please go to thermoscientific.com. Enter the product name (SOLA II) as the search term and click the Resources tab.
Page 200 THIS PAGE INTENTIONALLY BLANK Thermo Fisher Scientific SOLA II User Guide M-2...
Page 201: Appendix N Trace Level Measurements
Description of the SOLA II Trace The SOLA II Trace analyser is a modified version of the standard SOLA II, all characteristics of the SOLA II operation are applicable to the SOLA II Trace, it is available for both liquid and vapour samples;...
Page 202 The highest recommended range is a full scale of 5ppm, above this range the performance of the standard SOLA II is usually deemed sufficiently good to negate the benefits of the SOLA II Trace and provide a more cost effective solution, however users are invited to consult the factory for the implementation of ranges with the SOLA II Trace higher than 5ppm.
Page 203: Appendix O Vapour Sample Measurements
Appendix O: Vapour sample measurements Additional guidance on the SOLA II for Vapours This user manual contains information relating to the use of the SOLA II and SOLA II Trace for both liquid and vapour samples, this appendix provides additional guidance on the performance specification, ranges and technical characteristics for vapour samples, in particular samples that have a high dewpoint (Condensable Vapours).
Page 204 Figure O-1 SOLA II (CV) flow diagram SOLA II (CV) Hazardous area certifications Since the SOLA II (CV) is modified from the standard SOLA II analyser the hazardous area approvals may vary; please consult the factory for the latest approvals for installation in hazardous areas.
Page 205 Thermo Fisher Scientific 81 Wyman Street P.O. Box 9046 Waltham, Massachusetts 02454-9046 United States www.thermofisher.com...

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